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NMR Spectroscopy in Liquids and Solids provides an introduction of the general concepts behind Nuclear Magnetic Resonance (NMR) and its applications, including how to perform adequate NMR experiments and interpret data collected in liquids and solids to characterize molecule systems in terms of their structure and dynamics. The book is composed of ten chapters. The first three chapters consider the theoretical basis of NMR spectroscopy, the theory of NMR relaxation, and the practice of relaxation measurements. The middle chapters discuss the general aspects of molecular dynamics and their relationships to NMR, NMR spectroscopy and relaxation studies in solutions, and special issues related to NMR in solutions. The remaining chapters introduce general principles and strategies involved in solid-state NMR studies, provide examples of applications of relaxation for the determination of molecular dynamics in diamagnetic solids, and discuss special issues related to solid state NMR― including NMR relaxation in paramagnetic solids. All chapters are accompanied by references and recommended literature for further reading. Many practical examples of multinuclear NMR and relaxation experiments and their interpretations are also presented. The book is ideal for scientists new to NMR, students, and investigators working in the areas of chemistry, biochemistry, biology, pharmaceutical sciences, or materials science.

Physical Basis of Nuclear Magnetic Resonance Nuclei in the External Magnetic Field Radio-frequency Irradiation: Continuous Wave and Radio-frequency Pulses From Nuclear Relaxation to Shapes of NMR Signals Registration of NMR Signals: General Principles and NMR Equipment Enhancement of Sensitivity in NMR Experiments Two-Dimensional and Multi-Quantum NMR Experiments: General Aspects References and Recommended Literature Chemical Shift and Nuclear Coupling Theory and Practical Consequences Phenomenology of Chemical Shift Chemical Shifts in the Presence of Unpaired Electrons Spin-Spin Coupling Dipolar Coupling Quadrupolar Coupling References and Recommended Literature Nuclear Relaxation: Theory and Measurements Molecular Motions: Common Characteristics Mechanisms of Spin-Spin and Spin-Lattice Nuclear Relaxation Spin Diffusion in Solids Paramagnetic Relaxation Relaxation Time Measurements Experiments and Measurements: Errors, Problems, and Artifacts Artifacts in Relaxation Time Measurements References and Recommended Literature NMR and Molecular Dynamics: General Principles Kinetics of Chemical Reactions by NMR Spectroscopy Chemical Exchange Molecular Mobility from Relaxation Times NMR Relaxometry: Diffusion Coefficients Molecular Dynamics from Low-Field NMR References and Recommended Literature NMR Spectroscopy in Solutions: Practice and Strategies of Structural Studies Preparation of NMR Samples: Minimal Requirements Structural Studies by Solution NMR: General Strategies and 1D and 2D NMR Experiments Conformational (Isomeric) Analysis by NMR in Solutions NOE and Residual Dipolar Coupling Measurements in Structural Studies References and Recommended Literature NMR Relaxation in Solutions: Applications Partially Relaxed NMR Spectra: Resolving the Unresolved Signals and Assigning NMR Signals Relaxation Times in Solutions: Quadrupolar Coupling Constants and Chemical Shift Anisotropy NMR Relaxation and Intermolecular Interactions Solvent Relaxation Relaxation in Molecular Systems with Chemical Exchanges Structural Aspects Obtained from Relaxation in Solutions References and Recommended Literature Solution NMR: Special Issues Optical Isomers in NMR Spectra Solution NMR of Biomolecules: General Principles Dynamics in Liquids by NMR para-Hydrogen and NMR Spectroscopy in Solutions Solution NMR Spectroscopy and Heterogeneous Molecular Systems Free Radicals in NMR Spectra of Solutions References and Recommended Literature Solid-State NMR Spectroscopy: General Principles and Strategies Detection of NMR Signals in Solids General Approaches and Strategies of NMR Studies in Solids Increasing Spectral Resolution in Solid-State NMR Assignments of Signals Multinuclear Solid-State NMR Applications References and Recommended Literature Molecular Dynamics and Nuclear Relaxation in Solids: Applications Temperature Control and Calibration in Solid-State NMR Unusually Fast Molecular Dynamics in Solids Molecular Dynamics in Solids Determined by Full Line-Shape Analysis One- and Two-Dimensional Exchange NMR Spectroscopy in Solids: Slow Molecular Dynamics Dynamics in Solids by Cross-Polarization NMR Experiments Molecular Dynamics in Solids by NMR Relaxation Measurements: Common Aspects of Applications Dynamics in Heterogeneous and Disordered Solids: NMR Spectra and Relaxation Dispersion Dynamics in Solids under High Pressure References and Recommended Literature Solid-State NMR: Special Issues Solid-State NMR of Proteins Solid-State NMR in Metals and Alloys Porous Diamagnetic Solids: Porosity via NMR Experiments Solid-State NMR and Paramagnetic Molecular Systems Nuclear Relaxation in Paramagnetic Solids: Applications References and Recommended Literature Concluding Remark

Vladimir I. Bakhmutov works in the Department of Chemistry at Texas A&M University in College Station. He earned his PhD in physical inorganic chemistry from Moscow State University. Dr. Bakhmutov’s research interests include extensive applications of solution and solid state NMR techniques for chemistry, molecular physics, and materials science. Dr. Bakhmutov has been granted visiting professorships by Zurich University, Switzerland; Bourgogne University, Dijon, France; Rennes University, France; CINVESTAV, Mexico; and Iberdrola, Zaragosa, Spain. He is the author or co-author of more than 300 scientific articles and five books.

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